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Tag: technique

X-Ray Powder Diffraction

X-Ray Powder Diffraction

X-RAY POWDER DIFFRACTION is a process of identifying the crystal structure (i.e. atomic spacing) of a powder sample using x-rays. It can tell you both what elements are present as well as differentiating between polymorphs. PRODUCING X-RAYS Electrons are freed from a tungsten filament (aka cathode) by heating, where the valence electrons are free to move with very little energy input. Normally the electrons would stay within the metal because it becomes (+) charged when the electrons leave, drawing them…

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Gas Chromatography

Gas Chromatography

Gas Chromatography is a method of analyzing an unknown liquid mixture by separating the components by boiling point 1. A liquid mixture of unknown compounds A and B is injected into a column with an inert gas (usually Helium) which pushes the liquid through the column into an oven (brown) where it vaporizes 2. The column is coated with a liquid with a high boiling point (green). The gas with the higher boiling point (B) will form stronger bonds with…

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